標(biāo)準(zhǔn)編號(hào):	GB 5009.75-2014
中文名稱(chēng):	食品安全國(guó)家標(biāo)準(zhǔn) 食品添加劑中鉛的測(cè)定
英文名稱(chēng):	National Food Safety Standard—Determination of Lead in Food Additives
行業(yè)分類(lèi):	GB    國(guó)家標(biāo)準(zhǔn)
發(fā)布機(jī)構(gòu):	中華人民共和國(guó)國(guó)家衛(wèi)生和計(jì)劃生育委員會(huì)
發(fā)布日期:	2015-09-21
實(shí)施日期:	2016-3-21
標(biāo)準(zhǔn)狀態(tài):	valid
替代舊標(biāo)準(zhǔn):	GB/T 5009.75-2003 食品添加劑中鉛的測(cè)定
翻譯語(yǔ)言:	英文
文件格式:	PDF
中文字符數(shù):	8000 字
翻譯價(jià)格(元):	320.0
交付時(shí)間:	付款后 1 個(gè)工作日

1 Scope This standard specifies the limit test and quantitative test methods to determine the lead in food additives. This standard is applicable to the limit test and quantitative test on lead in food additives. Method I Diphenyl Thiocarbazone (Dithizone) Colorimetry 2 Principle Treat the sample by adding diammonium hydrogen citrate, potassium cyanide and hydroxylamine hydrochloride, etc., to eliminate the interference of ions such as iron, copper and zinc. At pH 8.5~9.0, the lead ion reacts with diphenyl thiocarbazone (dithizone) to generate red complex which is extracted with trichloromethane. Carry out limit test or quantitative test and compare with the standard series. 3 Reagents and Materials Note: unless otherwise specified, the reagents used in this method are analytically pure, and the water is Grade 1 water specified in GB/T 6682.

Contents Foreword i 1 Scope 2 Principle 3 Reagents and Materials 4 Apparatus 5 Preparation of Samples 6 Determination 7 Expression of Analysis Result 8 Precision 9 Miscellaneous 10 Principle 11 Reagents and Materials 12 Apparatus 13 Analysis Procedures 14 Expression of Analysis Results 15 Precision 16 Miscellaneous Appendix A Reference Conditions for Microwave Digestion